Tellurogermanate
Tellurogermanates or telluridogermanates are compounds with anions with tellurium bound to germanium. They are analogous with germanates, thiogermanates and selenidogermanates.[1]
Properties
Most tellurogermanates are coloured black. They are semiconductors with a small band gap.
Ge4Te104− forms an adamantane structure.[2]
List
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crystal
system
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space
group
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cell dimensions
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volume
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density
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ref
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(Et4N)4Ge4Te10
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cubic
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P43m
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a 22.923
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black
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[3][2]
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Na6Ge2Te6
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monoclinic
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P21/c
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a=8.899 b=12.946 c=8.908 β =119.87°
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[4]
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K2GeTe4
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monoclinic
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P21/c
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a = 12.703 b = 8.680 c = 9.829 β = 104.8°
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[5]
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K4Ge4Te10
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[2]
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K6Ge2Te6
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monoclinic
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C2/c
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[6]
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[K4(H2O)2][GeTe4]
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monoclinic
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C2/c
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a 19.43 b 7.4133 c 13.845 β 129.93°
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[7]
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Cr2Ge2Te6
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rhombohedral
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P312
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a=6.8275 c=20.5619 V=0 Z=3
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830
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6.091
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dark grey; ferromagnetic < 63K
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[8][9]
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[Mn(en)3]2(Ge5Te10)
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orthorhombic
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P21212
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a 10.735 b 23.417 c 8.932
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[10]
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(Me4N)2Mn[Ge4Te10]
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I4
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band gap 0.69 eV
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[11]
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Na9Sb[Ge2Te6]2
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monoclinic
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C2/c
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a = 9.541 b = 26.253 c = 7.582β = 122.23° Z = 2
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dark grey; band gap 1.51 eV
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[12]
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Cs2GeTe4
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848.8
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orthorhombic
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Pnma
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a=12.602 b=11.501 c=7.694 Z=4
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1113.8
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5.06
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[13]
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Cs6Ge2Te6
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monoclinic
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C2/c
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a = 17.027 b = 14.237 c = 10.104 β = 96.701° Z = 4
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black; Ge-Ge bond
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[6]
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Cs2Ge3Ga6Te14
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P3m1
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a = 8.2475 c = 14.2734 Z = 1
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840.82
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[14]
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Cs2Ge3In6Te14
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P3m1
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a =8.5404 c = 14.6766 Z = 1
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927.07
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[14]
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β-BaGa2Te4
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orthorhombic
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Imma
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a = 23.813 b = 11.967 c = 6.7215
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[15]
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Ba2GeTe3
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orthorhombic
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Pnma
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a = 6.790 b = 23.720 c = 6.930
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[16]
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Ba2Ge2Te5
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orthorhombic
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Pna21
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a= 13.3879 b= 9.1703 c= 9.9441 Z= 4
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black
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[17]
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Ba5Ga2Ge3Te12
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monoclinic
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P21/c
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a = 13.6540 b = 9.6705 c = 23.1134
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[15]
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Ba6In2Ge2Te15
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monoclinic
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P21/c
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a 9.6201 b 13.4225 c 27.585 β 92.469°
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[18]
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Ba4Ge2Sb2Te10
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monoclinic
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P21/c
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a = 13.984 b = 13.472 c = 13.569 β = 90.16° Z=4
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black
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[19]
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Tl2GeTe3
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orthorhombic
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Pnma
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a = 8.303 b = 21.514 c = 8.453 Z = 8
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black
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[20]
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Tl2GeTe5
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[21]
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References
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- ^ a b c Dhingra, Sandeep S.; Haushalter, Robert C. (January 1994). "An adamantane-like [Ge4Te10]4− anion: synthesis and single crystal structure determination of (Et4N)4[Ge4Te10]". Polyhedron. 13 (19): 2775–2779. doi:10.1016/S0277-5387(00)83436-1.
- ^ Herzog, Uwe; Rheinwald, Gerd (2001-12-01). "Novel Chalcogenides of Silicon with Bicyclo[2.2.2]octane Skeletons, MeSi(SiMe 2 E) 3 MR (E = S, Se, Te; M = Si, Ge, Sn; R = Me, Ph)". Organometallics. 20 (25): 5369–5374. doi:10.1021/om0105573. ISSN 0276-7333.
- ^ Eisenmann, Brigitte; Kieselbach, Emma; Schäfer, Herbert; Schrod, Heike (September 1984). "Über Thio-, Selenido- und Telluridogermanate (III): Zur Kenntnis von K6Ge2S6, K6Ge2Se6 und Na6Ge2Te6". Zeitschrift für anorganische und allgemeine Chemie (in German). 516 (9): 49–54. doi:10.1002/zaac.19845160908. ISSN 0044-2313.
- ^ Eisenmann, B.; Schrod, H.; Schäfer, H. (March 1984). "K2GeTe4, ein pertelluridogermanat mit kettenstruktur". Materials Research Bulletin (in German). 19 (3): 293–298. doi:10.1016/0025-5408(84)90169-7.
- ^ a b Friede, Bernd; Jansen, Martin (1999-08-01). "Darstellung und Kristallstruktur von Hexacaesium-hexatelluridodigermanat( III) (Cs 6 Ge 2 Te 6 )". Zeitschrift für Naturforschung B. 54 (8): 1095–1098. doi:10.1515/znb-1999-0819. ISSN 1865-7117. S2CID 101671292.
- ^ Melullis, Maike; Dehnen, Stefanie (October 2007). "Syntheses, Crystal Structures, UV-Vis Spectra and First NMR Spectra of New Potassium Salts of Chalcogenogermanates". Zeitschrift für anorganische und allgemeine Chemie (in German). 633 (13–14): 2159–2167. doi:10.1002/zaac.200700311.
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- ^ Zhang, Qichun; Armatas, Gerasimos; Kanatzidis, Mercouri G. (2009-09-21). "Activation of Tellurium with Zintl Ions: 1 / ∞ {[Ge 5 Te 10 ] 4− }, An Inorganic Polymer with Germanium in Three Different Oxidation States". Inorganic Chemistry. 48 (18): 8665–8667. doi:10.1021/ic901282g. ISSN 0020-1669. PMID 19685902.
- ^ Tsamourtzi, Konstantina; Song, Jung-Hwan; Bakas, Thomas; Freeman, Arthur J.; Trikalitis, Pantelis N.; Kanatzidis, Mercouri G. (2008-12-15). "Straightforward Route to the Adamantane Clusters [Sn 4 Q 10 ] 4− (Q = S, Se, Te) and Use in the Assembly of Open-Framework Chalcogenides (Me 4 N) 2 M[Sn 4 Se 10 ] (M = Mn II , Fe II , Co II , Zn II ) Including the First Telluride Member (Me 4 N) 2 Mn[Ge 4 Te 10 ]". Inorganic Chemistry. 47 (24): 11920–11929. doi:10.1021/ic801762h. ISSN 0020-1669. PMID 18998670.
- ^ Schwarzmüller, Stefan; Hoai‐Thuong Tran, Vu; Yang, Fangshun; Oeckler, Oliver (2019-08-30). "The Sodium Antimony Telluridogermanate(III) Na 9 Sb[Ge 2 Te 6 ] 2". Zeitschrift für anorganische und allgemeine Chemie. 645 (16): 1037–1042. doi:10.1002/zaac.201900158. ISSN 0044-2313. S2CID 226907957.
- ^ Sheldrick, W. S.; Schaaf, B. (1995-10-01). "Methanolothermale Synthese und Kristallstruktur von Diselenido- und Ditelluridogermanaten(IV) der Alkalimetalle K – Cs / M ethanolothermal Synthesis and Crystal Structure of Diselenido- and Ditelluridogerm anates(IV) of the Alkali Metals K – Cs". Zeitschrift für Naturforschung B. 50 (10): 1469–1475. doi:10.1515/znb-1995-1007. ISSN 1865-7117. S2CID 97624411.
- ^ a b Zhang, Cheng-Yi; Zhou, Liu-Jiang; Chen, Ling (2012-07-02). "Quaternary Tellurides with Different Valent Ge Centers: Cs 2 Ge 3 M 6 Te 14 (M = Ga, In)". Inorganic Chemistry. 51 (13): 7007–7009. doi:10.1021/ic300599q. ISSN 0020-1669. PMID 22702657.
- ^ a b Sun, Mengran; Zhang, Xingyu; Xing, Wenhao; Li, Zhuang; Liu, Wenhao; Lin, Zheshuai; Yin, Wenlong; Yao, Jiyong (2021-10-04). "Synthesis and Characterizations of Two Tellurides β-BaGa 2 Te 4 and Ba 5 Ga 2 Ge 3 Te 12 with Flexible Chain Structure". Inorganic Chemistry. 60 (19): 14793–14802. doi:10.1021/acs.inorgchem.1c02045. ISSN 0020-1669. PMID 34529425. S2CID 237546151.
- ^ Prakash, Jai; Mesbah, Adel; Lebègue, Sébastien; Ibers, James A. (November 2019). "Synthesis, crystal structure, and electronic structure of Ba2GeTe3(Te2)". Solid State Sciences. 97: 105974. Bibcode:2019SSSci..9705974P. doi:10.1016/j.solidstatesciences.2019.105974. S2CID 203129111.
- ^ Jana, Subhendu; Ishtiyak, Mohd; Govindaraj, Lingannan; Arumugam, Sonachalam; Tripathy, Bikash; Malladi, Sairam K.; Niranjan, Manish K.; Prakash, Jai (March 2022). "Metal to insulator transition in Ba2Ge2Te5: Synthesis, crystal structure, resistivity, thermal conductivity, and electronic structure". Materials Research Bulletin. 147: 111641. doi:10.1016/j.materresbull.2021.111641. S2CID 244111737.
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- ^ Klepp, Kurt O.; Ecker, Paul (July 1995). "The Crystal Structure of Tl2GeTe3: A Tellurogermanate(IV) with Bitetrahedral Anions". Journal of Solid State Chemistry. 117 (2): 351–355. Bibcode:1995JSSCh.117..351K. doi:10.1006/jssc.1995.1284.
- ^ Marsh, Richard E. (August 1990). "On the structure of Tl2GeTe5". Journal of Solid State Chemistry. 87 (2): 467–468. Bibcode:1990JSSCh..87..467M. doi:10.1016/0022-4596(90)90051-X.
Salts and covalent derivatives of the telluride ion |
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